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GEM

The GEneral Materials (GEM) powder diffractometer is a versatile instrument used to investigate the structure of crystalline and amorphous materials. GEM is also well-suited for magnetic and large unit cell structural investigations.

Technical information

Moderator  Liquid methane at 110 K 
Incident wavelength  ~0.1 to ~3.6 Å 
Incident flight path    17.0 m 
Secondary flight path  1.03 to 2.77 m 
Incident beam dimensions (max)  40 mm (h) x 15 mm (w) 
Detector coverage  3.86 steradians (7.27 m2) 
Detector 2θ range  5 – 171° 
Q range  0.1 – 60, at best 
ΔQ/Q (%)  4.7 – 0.34 (detector banks 1 – 6) 

 

Related resources

Sample environment

Equipment routinely used on GEM:

  • Automatic sample changer (20 positions, room temperature)
  • Furnace (RT to 1000°C)
  • Top-loading CCR (5 to 300 K)
  • He4 cryostat (2 to 300 K)

Non-standard sample environment:

  • Gas panel kits for continuous gas flow cell or static gas loading experiments.
  • High pressure cells

Recent publications

Instrument reference

All publications and datasets based on experiments using GEM should cite that the data is collected by DOI: 10.5286/isis.instrument.4207. Experiment DOIs follow the format 10.5286/ISIS.E.RBXXXXXXX, where XXXXXXX is the 7-digit experiment (RB) number and these can be viewed via the Data Gateway.

Reference publication: Results on disordered materials from the GEneral Materials diffractometer, GEM, at ISIS, Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, 551, 1, 2005, 88-107. DOI: 10.1016/j.nima.2005.07.053.